Thermal behaviour of some metal complexes of N,N-diethyl-N'-benzoyl thiourea

Merdivan M., Aygun R., Kulcu N.

JOURNAL OF THERMAL ANALYSIS, vol.48, no.6, pp.1423-1429, 1997 (SCI-Expanded) identifier identifier

  • Publication Type: Article / Article
  • Volume: 48 Issue: 6
  • Publication Date: 1997
  • Doi Number: 10.1007/bf01983453
  • Journal Name: JOURNAL OF THERMAL ANALYSIS
  • Journal Indexes: Science Citation Index Expanded (SCI-EXPANDED), Scopus
  • Page Numbers: pp.1423-1429
  • Keywords: complexes, N,N-diethyl-N'-benzoylthiourea, thermal behaviour
  • Middle East Technical University Affiliated: Yes

Abstract

The thermal behaviour of the complexes of N,N-diethyl-N'-benzoylthiourea (DEBT) with NI(II), Cu(II), Pt(II), Pd(II) and Ru(III) was studied using differential thermal analysis (DTA) and thermogravimetry (TG). These complexes undergo only a pyrolytic decomposition process. A gas chromatography-mass spectrometry combined system was used for the verification of the first decomposition product and X-ray diffraction method for the characterization of the final products of pyrolysis.